Preparation and Characterization of Pure Pla Filament and Pbat-Reinforced Pla Filament For Fdm 3d Printing / (Record no. 607408)

000 -LEADER
fixed length control field 02980nam a22001577a 4500
082 ## - DEWEY DECIMAL CLASSIFICATION NUMBER
Classification number 670
100 ## - MAIN ENTRY--PERSONAL NAME
Personal name Naeem Ul Hassan
245 ## - TITLE STATEMENT
Title Preparation and Characterization of Pure Pla Filament and Pbat-Reinforced Pla Filament For Fdm 3d Printing /
Statement of responsibility, etc. Naeem Ul Hassan
264 ## - PRODUCTION, PUBLICATION, DISTRIBUTION, MANUFACTURE, AND COPYRIGHT NOTICE
Place of production, publication, distribution, manufacture Islamabad :
Name of producer, publisher, distributor, manufacturer SMME- NUST;
Date of production, publication, distribution, manufacture, or copyright notice 2023.
300 ## - PHYSICAL DESCRIPTION
Extent 77p.
Other physical details Soft Copy
Dimensions 30cm
500 ## - GENERAL NOTE
General note This study focuses on preparing pure polylactic acid (PLA) and polybutylene adipate –coterephthalate (PBAT)-reinforced PLA filaments. PLA and PBAT are biodegradable aliphatic<br/>polyesters and have recently received considerable attentions. Due to its brittle nature, PLA has<br/>limited application in various fields. To overcome this challenge, numerous efforts have been made<br/>to incorporate various additives to enhance its performance. In this work, pure PLA filament and<br/>PBAT-reinforced PLA filament with diameter 1.75 ± 0.02 mm were prepared in the lab. Their<br/>thermal and mechanical properties were analyzed and compared with the commercial PLA<br/>filament bought from the market. Following the previous research works and suggestions of<br/>incorporating no more than 10 wt.% PBAT, we have mixed 8 wt.% PBAT into the PLA mixture.<br/>We then proceeded to extrude pure PLA and PBAT-reinforced PLA filaments at a temperature<br/>range of 170 oC to 180 oC, utilizing single screw extruder. Next, we printed tensile and flexural<br/>specimens using an FDM 3D printer, in accordance with Taguchi L9 OA. Due to PBAT’s high<br/>ductility, 92-8 wt.% PLA-PBAT filament demonstrated a significant increase in elongation at<br/>break, reaching up to 12%. Likewise, the PLA-PBAT filament displayed tensile and flexural<br/>strengths of up to 48.34 MPa and 107.295 MPa respectively. These values are comparable to the<br/>tensile and flexural strengths of pure PLA, which is a great indication that the addition of 8 wt.%<br/>PBAT did not cause any unacceptable reduction in the tensile and flexural strengths. Additionally,<br/>it was found through DSC analysis that PLA-PBAT filament exhibited a higher degree of<br/>crystallinity (Xc) of up to 38.7%, which is significantly higher than that of pure extruded PLA.<br/>Furthermore, the TGA curve indicated that thermal stability of PLA-PBAT filament was improved<br/>by adding 8 wt.% PBAT. Moreover, digital microscopy results revealed that PLA-PBAT filament<br/>had a ductile fracture after necking, whereas pure PLA had a brittle fracture. Lastly, statistical<br/>analysis showed that both material type and layer thickness had significant impact on the results.<br/>The addition of this new PLA-PBAT filament provides an additional alternative to the current<br/>FDM filaments, and it will aid in reducing the constraints of the materials when it comes to additive<br/>manufacturing (AM) progress.
650 ## - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element MS Design and Manufacturing Engineering
700 ## - ADDED ENTRY--PERSONAL NAME
Personal name Supervisor : Dr. Shahid Ikramullah Butt
856 ## - ELECTRONIC LOCATION AND ACCESS
Uniform Resource Identifier <a href="http://10.250.8.41:8080/xmlui/handle/123456789/33850">http://10.250.8.41:8080/xmlui/handle/123456789/33850</a>
942 ## - ADDED ENTRY ELEMENTS (KOHA)
Source of classification or shelving scheme
Koha item type Thesis
Holdings
Withdrawn status Permanent Location Current Location Shelving location Date acquired Full call number Barcode Koha item type
  School of Mechanical & Manufacturing Engineering (SMME) School of Mechanical & Manufacturing Engineering (SMME) E-Books 01/16/2024 670 SMME-TH-852 Thesis
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