Development and Characterization of Graphene Oxide Induced Alumina Composite Using Powder Metallurgy (Record no. 612916)

000 -LEADER
fixed length control field 02671nam a22001577a 4500
082 ## - DEWEY DECIMAL CLASSIFICATION NUMBER
Classification number 670
100 ## - MAIN ENTRY--PERSONAL NAME
Personal name Abuzar
245 ## - TITLE STATEMENT
Title Development and Characterization of Graphene Oxide Induced Alumina Composite Using Powder Metallurgy
Statement of responsibility, etc. Abuzar
264 ## - PRODUCTION, PUBLICATION, DISTRIBUTION, MANUFACTURE, AND COPYRIGHT NOTICE
Place of production, publication, distribution, manufacture Islamabad :
Name of producer, publisher, distributor, manufacturer SMME- NUST;
Date of production, publication, distribution, manufacture, or copyright notice 2025.
300 ## - PHYSICAL DESCRIPTION
Extent 124p.
Other physical details Soft Copy
Dimensions 30cm
500 ## - GENERAL NOTE
General note Graphene oxide (GO)-reinforced alumina (Al2O3) composites have garnered significant<br/>attention for aerospace applications due to their enhanced mechanical properties. This<br/>study investigates the synthesis, sintering behaviour, and mechanical characterization<br/>of GO-alumina composites fabricated using powder metallurgy. GO concentrations of<br/>0.5, 0.9, and 1.2 wt.% were incorporated into an alumina matrix and processed via<br/>uniaxial cold pressing at 450 MPa, followed by liquid-phase sintering at 1500°C and<br/>1550°C for dwell times of 60 and 90 minutes.<br/>Material characterization through X-ray diffraction (XRD) confirmed the presence of<br/>beta or gamma alumina, while Raman spectroscopy demonstrated the structural<br/>integrity of GO within the composite. Scanning electron microscopy (SEM) revealed a<br/>uniform dispersion of GO at lower concentrations but agglomeration at 1.2 wt.%,<br/>adversely affecting densification and mechanical performance. The relative density of<br/>the composites decreased with increasing GO content due to the formation of porous<br/>regions and weak interfacial bonding. The highest relative density (91.45%) was<br/>observed in pure alumina sintered at 1550°C for 90 minutes, while GO-reinforced<br/>samples exhibited reduced densification efficiency. Vickers microhardness testing<br/>indicated peak hardness at 0.5 wt.% GO, reaching 1838 HV at 1550°C for 90 minutes.<br/>However, higher GO content (>0.9 wt.%) led to a decline in hardness due to increased<br/>porosity and structural defects.<br/>The research finding indicate the potential of GO-alumina composites for aerospace<br/>applications but also underscores the limitations of conventional liquid-phase sintering<br/>in achieving optimal densification and mechanical properties. Compared to Spark<br/>Plasma Sintering (SPS), which provides rapid heating, improved grain refinement, and<br/>reduced porosity, the current processing method resulted in lower densification and<br/>increased defect formation. Future work should explore SPS to mitigate agglomeration,<br/>enhance densification efficiency, and improve the overall performance of GO-alumina<br/>composites.
650 ## - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element MS Design and Manufacturing Engineering
700 ## - ADDED ENTRY--PERSONAL NAME
Personal name Supervisor : Dr. Sadaqat Ali
856 ## - ELECTRONIC LOCATION AND ACCESS
Uniform Resource Identifier <a href="http://10.250.8.41:8080/xmlui/handle/123456789/49856">http://10.250.8.41:8080/xmlui/handle/123456789/49856</a>
942 ## - ADDED ENTRY ELEMENTS (KOHA)
Source of classification or shelving scheme
Koha item type Thesis
Holdings
Withdrawn status Permanent Location Current Location Shelving location Date acquired Full call number Barcode Koha item type
  School of Mechanical & Manufacturing Engineering (SMME) School of Mechanical & Manufacturing Engineering (SMME) E-Books 02/19/2025 670 SMME-TH-1113 Thesis
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